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Ketone-Directed Cobalt(III)-Catalyzed Regioselective C2 Amidation of Indoles

Xinxia Shi, Wei‐Yan Xu, Rongchao Wang, Xiaofei Zeng, Huayu Qiu, Min Wang

2020The Journal of Organic Chemistry34 citationsDOI

Abstract

An efficient cobalt(III)-catalyzed method for the direct C-H amidation of unprotected indoles for 2-amino indole scaffold construction has been developed. With dioxazolone as the amidating reagent, a variety of 2-amino indole derivatives were achieved in moderate to excellent yields using an organic acid as the additive and a ketone as the directing group.

Topics & Concepts

ChemistryKetoneCobaltIndole testRegioselectivityReagentCatalysisOrganic chemistryCombinatorial chemistryAmino acidBiochemistryCatalytic C–H Functionalization MethodsSynthesis and Catalytic ReactionsSulfur-Based Synthesis Techniques
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