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Influence of inorganic scale formation on asphaltene behavior during water injection

Mohammad Amin Behnam Motlagh, Amir Hossein Saeedi Dehaghani

2025Scientific Reports5 citationsDOIOpen Access PDF

Abstract

This study presents significant advances in understanding the complex interplay between inorganic scaling and asphaltene behavior in oil–water systems through innovative experimental and analytical approaches. We aim to elucidate non-linear, concentration-dependent scaling phenomena, molecular-level asphaltene transformations during scaling, and the coupled impacts on interfacial properties. To that end, we conducted carefully designed static incompatibility tests using formation waters (FWs) containing Ba 2+ or Sr 2+ and modified seawater (SW) with controlled sulfate (4 × Na 2 SO 4 ), quantified precipitates and characterized them by energy dispersive X-ray spectroscopy (EDS)/X-ray diffraction (XRD), tracked molecular signatures by Fourier transform infrared spectroscopy (FTIR), and monitored polarity indices and interfacial tension (IFT). The results show that sulfate concentration thresholds govern scaling; at 4 × Na 2 SO 4 , Sr 2+ systems yield 85.43% gypsum with 14.57% halite, whereas Ba 2+ systems form 75.08% gypsum and 24.92% barite, confirming barium’s stronger scaling tendency. Polarity indices shift from 0.1296 (crude oil) to 0.1515 (a non-scaling Sr 2+ condition) and then decrease to 0.1388 under scaling, with more pronounced effects in Ba 2+ systems; EDS indicates sequestration of oxygen and sulfur heteroatoms within scale matrices. Consistently, IFT rises from 27.33 to 39.04 mN/m in Sr 2+ systems and from 33.41 to 42.73 mN/m in Ba 2+ systems under scaling. These findings provide a quantitative framework for predicting and managing coupled scaling–asphaltene interactions in carbonate reservoirs and enable optimized water-injection strategies that jointly control scale formation and enhance oil recovery, improving on conventional approaches that treat these challenges separately.

Topics & Concepts

AsphalteneScalingGypsumCarbonateSulfateChemical engineeringFourier transform infrared spectroscopySulfurMaterials scienceHeteroatomSpectroscopyChemistrySeawaterDissolutionSurface tensionEnhanced oil recoveryPetroleumEnvironmental scienceScale (ratio)Yield (engineering)Infrared spectroscopyFlux (metallurgy)Formation waterFiltration (mathematics)DiffractionPetroleum Processing and AnalysisEnhanced Oil Recovery TechniquesCalcium Carbonate Crystallization and Inhibition
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