The fabrication of a novel polyacrylonitrile/reduced graphene oxide-amino-halloysite/bimetallic metal–organic framework electrospun nanofiber adsorbent for the ultrasonic-assisted thin-film microextraction of fatty acid methyl esters in dairy products with gas chromatography-flame ionization detection

Abstract

. The relative standard deviations for intra-day and inter-day precision were 2.4-4.7% and 2.6-3.4%, respectively. In the present work, the UA-TFME method was successfully applied for the quantification of fatty acid methyl esters in dairy products (milk, yogurt, cheese, yogurt soda and butter samples) for the first time. The fatty acids were transesterified using standard procedures and were subjected to UA-TFME treatment prior to GC-FID determination. The developed method possesses the advantages of simplicity, rapidity, cost-effectiveness, sensitivity, and non-invasiveness.

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