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In-situ growth of NiS-Ni3S4 on dual-ligand Co-MOF as a new electrode for high-performance supercapacitors

Amir Hossein Alipour, Mohammad Soleimani Lashkenari, Mohsen Ghorbani, Leila Asadi Kafshgari

2025Scientific Reports11 citationsDOIOpen Access PDF

Abstract

Nowadays, new electrode materials for energy storage devices like mixed ligands and bi-metal MOFs have attracted a lot of attention owing to their high porosity and high capacity for charge storage. In this study, a Co-based metal-organic framework (4,4’-bpy = 4,4′-Bipyridine and H 3 BTC = 1,3,5-Benzenetricarboxylic acid) was successfully fabricated by a hydrothermal method. To obtain good electrochemical behavior, Co-MOFs were modified using a porous spherical scaffold of NiS/Ni 3 S 4 nanoparticles. The electrochemical efficiency was analyzed by electrochemical impedance spectroscopy, cyclic voltammetry, and galvanostatic charge-discharge methods. Detailed electrochemical scrutiny performed by Co-MOF/NiS-Ni 3 S 4 in a 6 M KOH electrolyte reveals a high specific capacity of 136.67 mAh/g at 1 A/g, with a superb cycle life of 91%. Co-MOF/NiS-Ni 3 S 4 //AC asymmetric supercapacitor produces a large amount of energy density (33.32 Wh/kg) and power density (600 W/kg). The produced composite is an appropriate candidate for electrodes in both batteries and hybrid supercapacitors, owing to its favorable electrochemical characteristics.

Topics & Concepts

SupercapacitorMaterials scienceElectrochemistryElectrodeElectrolytePorosityPower densityEnergy storageCapacitanceComposite numberNanotechnologyElectrochemical energy storageHydrothermal circulationChemical engineeringDielectric spectroscopyElectrochemical energy conversionCurrent densitySpecific energyEnergy densityElectrical impedanceScaffoldSupercapacitor Materials and FabricationMetal-Organic Frameworks: Synthesis and ApplicationsAdvancements in Battery Materials