Litcius/Paper detail

(001)-Oriented Sr:HfO<sub>2</sub>Ferroelectric Films Deposited by a Flexible Chemical Solution Method

Miguel Badillo, Sepide Taleb, Brenda Carreño-Jiménez, Taraneh Mokabber, R. Castanedo‐Pérez, G. Torres‐Delgado, Beatriz Noheda, Mónica Acuautla

2024ACS Applied Electronic Materials11 citationsDOIOpen Access PDF

Abstract

High Resolution Image Download MS PowerPoint Slide Remnant polarization values of ferroelectric HfO 2 -based films depend on proper control of the polar orthorhombic phase crystallization and the orientation of the polar domains. Most of the best quality films reported so far are (111)-oriented. While the largest polarization is expected in (001)-oriented films, with the polar axis out of the plane, such orientation is far less common. This paper demonstrates that highly (001)/(010)-oriented heterostructures of Sr:HfO 2 on Pt(111)-buffered Si can be attained in layered films deposited by a recently reported chemical solution deposition route. The oriented films display the short c -axis out of plane, giving place to a longer a lattice in plane. By tailoring the duration of rapid thermal processing, such oriented films produce highly ferroelectric, leakage-free capacitors. After wake-up cycling, a remnant polarization of 17 μC/cm 2, which is the highest reported for this dopant and technique, was achieved. Even though optimization is still needed to improve the electrical cyclability, our facile approach produces high- k, highly oriented Sr:HfO 2 films, through chemical deposition and annealing, and shows that the crystal orientations and phase purity of HfO 2 -based films can be further optimized by cost-effective chemical methods.

Topics & Concepts

FerroelectricityOrthorhombic crystal systemMaterials scienceChemical bath depositionPolarization (electrochemistry)CrystallizationAnnealing (glass)DopantHeterojunctionDielectricCrystal structureOptoelectronicsChemical engineeringThin filmNanotechnologyDopingCrystallographyChemistryComposite materialEngineeringPhysical chemistryFerroelectric and Negative Capacitance DevicesSemiconductor materials and devicesMXene and MAX Phase Materials