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Adducts of the Parent Boraphosphaketene H<sub>2</sub>BPCO and their Decarbonylative Insertion Chemistry

Stephan Hagspiel, Felipe Fantuzzi, Rian D. Dewhurst, Annalena Gärtner, Felix Lindl, Anna Lamprecht, Holger Braunschweig

2021Angewandte Chemie International Edition30 citationsDOIOpen Access PDF

Abstract

Abstract The first examples of Lewis base adducts of the parent boraphosphaketene (H 2 B‐PCO) and their cyclodimers are prepared. One of these adducts is shown to undergo mild decarbonylation and phosphinidene insertion into a B−C bond of a borole, forming very rare examples of 1,2‐phosphaborinines, B/P isosteres of benzene. The strong donor properties of these 1,2‐phosphaborinines are confirmed by the synthesis of their π complexes with the Group 6 metals.

Topics & Concepts

AdductChemistryOrganic chemistrySynthesis and characterization of novel inorganic/organometallic compoundsOrganophosphorus compounds synthesisCoordination Chemistry and Organometallics