Litcius/Paper detail

NORD: NO Relaxation Delay NMR Spectroscopy

Tamás Milán Nagy, Katalin E. Kövér, Ole W. Sørensen

2021Angewandte Chemie International Edition26 citationsDOIOpen Access PDF

Abstract

Abstract The novel concept of NORD ( NO r elaxation d elay) NMR spectroscopy is introduced. The idea is to design concatenated experiments in a way that the magnetization used in the first relaxes toward equilibrium during the second and vice versa, thus saving instrument time. Applications include complete well‐resolved 1 H‐ 1 H and 1 H‐ 13 C one‐bond and long‐range correlation maps of an 80 mM solution of a trisaccharide recorded in less than two minutes and hydrocortisone with extensive spectral overlap.

Topics & Concepts

Nuclear magnetic resonance spectroscopyRelaxation (psychology)SpectroscopyTransverse relaxation-optimized spectroscopyNuclear magnetic resonanceChemical physicsMaterials scienceChemistryFluorine-19 NMRComputational chemistryPhysicsQuantum mechanicsMedicineInternal medicineNMR spectroscopy and applicationsAdvanced NMR Techniques and ApplicationsAdvanced MRI Techniques and Applications