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What is the Real Origin of the Activity of Fe–N–C Electrocatalysts in the O<sub>2</sub> Reduction Reaction? Critical Roles of Coordinating Pyrrolic N and Axially Adsorbing Species

Xu Hu, Suya Chen, Letian Chen, Yun Tian, Sai Yao, Zhengyu Lu, Xu Zhang, Zhen Zhou

2022Journal of the American Chemical Society300 citationsDOI

Abstract

Fe–N–C electrocatalysts have emerged as promising substitutes for Pt-based catalysts for the oxygen reduction reaction (ORR). However, their real catalytic active site is still under debate. The underlying roles of different types of coordinating N including pyridinic and pyrrolic N in catalytic performance require thorough clarification. In addition, how to understand the pH-dependent activity of Fe–N–C catalysts is another urgent issue. Herein, we comprehensively studied 13 different N-coordinated FeNxC configurations and their corresponding ORR activity through simulations which mimic the realistic electrocatalytic environment on the basis of constant-potential implicit solvent models. We demonstrate that coordinating pyrrolic N contributes to a higher activity than pyridinic N, and pyrrolic FeN4C exhibits the highest activity in acidic media. Meanwhile, the in situ active site transformation to *O-FeN4C and *OH-FeN4C clarifies the origin of the higher activity of Fe–N–C in alkaline media. These findings can provide indispensable guidelines for rational design of better durable Fe–N–C catalysts.

Topics & Concepts

ChemistryCatalysisRational designCombinatorial chemistrySolventRedoxOxygen reductionOxygen reduction reactionReduction (mathematics)Inorganic chemistryNanotechnologyElectrochemistryOrganic chemistryPhysical chemistryElectrodeGeometryMathematicsMaterials scienceElectrocatalysts for Energy ConversionFuel Cells and Related MaterialsAdvanced Photocatalysis Techniques