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Organocatalytic enantioselective reaction of tertiary α-(7-indolyl)methanols with tryptamines

Zhibin Yue, Boming Shen, Jie Cao, Xuling Chen, Fang Fang, Pengfei Li, Peiyuan Yu, Wenjun Li

2023Organic Chemistry Frontiers27 citationsDOI

Abstract

With the aid of chiral phosphoric acid, enantioselective 1,6-addition of tryptamines to in situ formed alkynyl 7-methylene-7 H -indoles from tertiary α-(7-indolyl)methanols has been established, furnishing axially chiral tetrasubstituted allenes in high yields.

Topics & Concepts

TryptaminesChemistryEnantioselective synthesisPhosphoric acidMethyleneOrganic chemistryOrganocatalysisBrønsted–Lowry acid–base theoryStereochemistryCatalysisTryptamineBiochemistryAxial and Atropisomeric Chirality SynthesisSynthesis of Indole DerivativesAsymmetric Synthesis and Catalysis
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