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Nickel-Catalyzed C(sp<sup>3</sup>)–Sb Coupling of Chlorostibines with Unactivated Alkyl Chlorides and In Vitro Anticancer Activity of Products

Liyuan Le, Mingming Yin, Huifan Zeng, Wuxing Xie, Wenjun Zhou, Yi Chen, Biquan Xiong, Shuang‐Feng Yin, Nobuaki Kambe, Renhua Qiu

2023Organic Letters11 citationsDOI

Abstract

)-Sb coupling of unactivated alkyl chlorides with chlorostibines. This approach is highly versatile, tolerating various functional groups such as acetal, alkene, nitrile, amine, ester, silyl ether, thioether, and various heterocyclic compounds. Notably, the late-stage modification of bioactive molecules and the satisfactory anticancer activity against cancerous MDA-MB-231 also demonstrate the potential application.

Topics & Concepts

ChemistryThioetherNitrileAlkeneAlkylCatalysisNickelEtherSilylationAcetalMoleculeAmine gas treatingCombinatorial chemistryOrganic chemistryMedicinal chemistryCatalytic C–H Functionalization MethodsCatalytic Cross-Coupling ReactionsFluorine in Organic Chemistry
Nickel-Catalyzed C(sp<sup>3</sup>)–Sb Coupling of Chlorostibines with Unactivated Alkyl Chlorides and In Vitro Anticancer Activity of Products | Litcius