Litcius/Paper detail

Iron-Catalyzed Cross-Coupling Reactions Tuned by Bulky <i>Ortho</i>-Phenylene Bisphosphine Ligands

Laksmikanta Adak, Takuji Hatakeyama, Masaharu Nakamura

2021Bulletin of the Chemical Society of Japan20 citationsDOIOpen Access PDF

Abstract

Abstract The significant progress made in the context of iron-catalyzed cross-coupling reactions in the past several years has boosted competition with well-known nickel and palladium catalyst systems. Iron-catalyzed protocols not only benefit from economic and toxicology standpoints, but also exhibit a range of reactivities and tolerate many functional groups. To date several iron catalyst systems have been developed, ranging from the use of simple iron salts to more complex stoichiometric/catalytic modifiers. Effective N-heterocyclic carbenes and bisphosphine ligands have also been developed for the cross-coupling reactions of organic electrophiles using diverse organometallic reagents. Indeed, the use of bisphosphine ligands in the field of iron-catalyzed cross-coupling reactions is important for new applications in modern synthetic organic chemistry. This account summarizes the recent developments in practical and novel iron-catalyzed cross-coupling reactions employing bulky o-phenylene bisphosphine ligands and their mechanistic views.

Topics & Concepts

ChemistryCatalysisElectrophileReagentCoupling reactionCombinatorial chemistryPhenyleneContext (archaeology)Organic synthesisTransmetalationLigand (biochemistry)Organic chemistryPolymerReceptorBiochemistryBiologyPaleontologyCatalytic Cross-Coupling ReactionsCatalytic C–H Functionalization MethodsCyclopropane Reaction Mechanisms