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Gallic acid-iron complex modified magnesium hydroxide and its effect on flame retardancy of EVA

Tao Wang, Dongwei Yao, Guang‐Zhong Yin, Yan Jiang, Na Wang, De‐Yi Wang

2022Advanced Industrial and Engineering Polymer Research13 citationsDOIOpen Access PDF

Abstract

In this paper, a green method of modifying high flame retardant and high mechanical properties MH was proposed, gallic acid (GA)-Fe3+ complex was employed to modify the surface of magnesium hydroxide (MH), aiming to achieve novel functionalized MH-based flame retardant for ethylene-vinyl acetate copolymer (EVA). The structural and morphological characterization of the newly designed flame retardant were studied by Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy, Scanning electron microscope and X-ray Diffraction. The flame retardancy of EVA, EVA/MH, EVA/[email protected] was investigated via Limiting oxygen index, UL-94 vertical combustion tests, and cone calorimeter test. The LOI and UL94 results showed that EVA/[email protected] (01) achieved an LOI of 38.5% and UL-94 passed the V-0 grade. The CCT results showed that compared with neat EVA, the peak heat release rate (pHRR) of EVA/[email protected] decreased by 90.83%, and TSP decreased by 86%, as compared to neat EVA. The mechanical properties of EVA/MH, EVA/[email protected] were investigated via tensile and impact tests. Compared with EVA/MH, [email protected] shows good tensile property and impact resistance, the impact strength of EVA/[email protected] increased by more than 28%, and the elongation at break increased by 145%.

Topics & Concepts

Limiting oxygen indexCone calorimeterMaterials scienceEthylene-vinyl acetateFire retardantUltimate tensile strengthFourier transform infrared spectroscopyThermal stabilityComposite materialScanning electron microscopeMagnesiumNuclear chemistryChemical engineeringCopolymerPyrolysisChemistryPolymerMetallurgyCharEngineeringFlame retardant materials and propertiesMagnesium Oxide Properties and ApplicationsElectromagnetic wave absorption materials
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