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Evolution of microstructure and intervariant boundaries of α phase in electron beam melted and heat‐treated Ti–6Al–4V alloy

Ming Wang, Haoqing Li, Hong Guo, Feng Liu, Shu-Yu Liu, Xiaoying Fang

2020Rare Metals22 citationsDOI

Abstract

Abstract It is important to understand the correlation between grain morphology and intervariant boundaries of the α phase after heat treatment below β transus of the electron beam melted (EBMed) Ti–6Al–4V alloy. Scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD) analysis have shown about 99% α phase and 1% β phase in the heat‐treated samples when the temperature rises to 950 °C. Four distinct types of α grain morphology have been found: allotromorphous α, relatively coarse α plate, large precipitation α and granular α. A single peak of the intervariant boundary with the misorientation of 60°/ associated with Burgers orientation relationship (OR) was found in the allotromorphous α colony. Multiple intervariant boundaries mixed with a fraction of general high‐angle grain boundary (GHABs, not Burgers OR) were present in the relatively coarse α plate colony. Almost only low‐angle grain boundaries (LABs) with the misorientation of < 5° were found in the large precipitation α grains. β phase tends to distribute around the boundaries of relatively coarse α plates. It suggests that different formation mechanisms are involved in the distinct types of α grain morphology.

Topics & Concepts

MisorientationMaterials scienceElectron backscatter diffractionGrain boundaryMicrostructurePrecipitationAlloyPhase (matter)Grain boundary strengtheningScanning electron microscopeElectron diffractionDiffractionCondensed matter physicsCrystallographyComposite materialOpticsChemistryPhysicsOrganic chemistryMeteorologyAdditive Manufacturing Materials and ProcessesTitanium Alloys Microstructure and PropertiesMetal and Thin Film Mechanics
Evolution of microstructure and intervariant boundaries of α phase in electron beam melted and heat‐treated Ti–6Al–4V alloy | Litcius