Litcius/Paper detail

Trinuclear Organometallic Pt−Ir−Pt Complexes: Insights into Photophysical Properties, Amino Acid Binding and Protein Sensing

Bishnu Das, Parna Gupta

2021Chemistry - An Asian Journal16 citationsDOI

Abstract

Abstract The rational synthesis of trinuclear emissive organometallic complexes with two equivalent platinum(II) centres appended to the ancillary substituted 2,2′‐bipyridyl ligand of the cyclometalated iridium(III) centre is reported here. The alkynyl‐platinum moiety and cyclometalated iridium(III) centres have been separated through a non‐conjugated CH 2 −O−CH 2 linkage. The emission titration with amino acids reveals that the complexes sense free amino acids. The luminescence sensing of BSA is thus attributed to the amino acid sensing ability of the complexes and confirmed by emission anisotropy and Far‐UV CD spectral study. The decrease in α‐helix in the CD spectra signifies the changes in the secondary structure of protein in presence of the complexes.

Topics & Concepts

IridiumMoietyChemistryPlatinumTitrationAmino acidLuminescenceLigand (biochemistry)StereochemistryCrystallographyPhotochemistryInorganic chemistryCatalysisMaterials scienceOrganic chemistryBiochemistryReceptorOptoelectronicsMetal complexes synthesis and propertiesOrganic Light-Emitting Diodes ResearchLanthanide and Transition Metal Complexes