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Nickel-catalyzed reductive monofluoroakylation of alkyl tosylate with bromofluoromethane to primary alkyl fluoride

Ru Cui, Jie Sheng, Bingbing Wu, Duo‐Duo Hu, Hong-Qian Zheng, Xi‐Sheng Wang

2021Chemical Communications26 citationsDOI

Abstract

A nickel-catalysed direct terminal monofluoromethlyation between alkyl tosylates and a low-cost, industrial raw material bromofluoromethane has been developed. This transformation has demonstrated high efficiency, mild conditions, and good functional-group compatibility. The key to success of this transformation lies in the ligand and mild base selection, ensuring the generation of various terminal monofluormethylation products.

Topics & Concepts

AlkylCatalysisNickelChemistryPrimary (astronomy)FluorideMedicinal chemistryOrganic chemistryInorganic chemistryPhysicsAstronomyFluorine in Organic ChemistryInorganic Fluorides and Related Compounds
Nickel-catalyzed reductive monofluoroakylation of alkyl tosylate with bromofluoromethane to primary alkyl fluoride | Litcius